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8% and 95.8%, but no precipitate was found in 1.0-10 mM oxalate-Cr-NaBH4 systems. This is related to whether there was a sufficient oxalate dosage, which could be complexed with Cr (III) at a molar ratio of 11. The precipitates were analysed by means of electron spin resonance (ESR), atomic force microscopy (AFM), X-ray diffraction (XRD), and Fourier transform infrared spectroscopy (FTIR), indicating that Cr (III) could support oxalate coprecipitation. The results of the present study reveal the influence of oxalate on Cr(