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Scanning electron microscopy (SEM) confirmed the efficient encapsulation of SiNP inside nano-fibers (200-400 nm), contingent upon the precise amount of material used. The encapsulating materials were subjected to a carbonization process at 755 degrees Celsius, creating a Si-O-C material with varying SiNP content in the samples, exemplified by Si@C-SiNF-5 and Si@C-SiNF-10. SEM and X-ray
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