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Experiments performed within living organisms confirmed the remarkable therapeutic effectiveness and insignificant systemic harm of PS@Cu9S8 nanocatalysts. The study not only produced a superior multifunctional nanocatalyst for the synergistic treatment of tumors via photothermal and chemodynamic approaches, but it also presented a simple method for designing high-performance agents for cancer therapy. Na2MgScF7 (NMSF) was experimentally synthesized for the first ti