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Fluorescence monitoring of guanidinium chloride-induced unfolding reveals that superstructure-associated cyt.c is stabilized to unfolding before and after chemical reduction of FeIII-cyt.c to form FeII-cyt.c, indicating that the superstructures remain intact during microheterogeneous redox reactions. Smaller nucleating Au nanoparticles or lower ionic strength in the buffered medium yields a greater extent of cyt.c reduction. Partial oxidation of the cyt.c-associated nanoparticulate Au is verified by X-ray photoelectron spectroscopy. Th
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