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Accurate double-blind identification of unknown samples using the proposed sensor array was also demonstrated, indicating its reliability for practical practice. In this study, a facile one step solvo-thermal procedure has been employed in generating magnetite-silver core-shell nanocomposites (AgNPs@ Fe3O4) with superior peroxidase-like catalytic property than bare magnetic nanoparticles (Fe3O4). The composites were characterized using different techniques such as transmission electron microscopy (TEM), scanning electron microscopy (SEM)